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Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides
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Cook, Daniel Sean, Wu, Yue, Lienau, Karla, More, Rene, Kashtiban, Reza J., Magdysyuk, Oxana V., Patzke, Greta R. and Walton, Richard I. (2017) Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides. Chemistry of Materials, 29 (12). pp. 5053-5057. doi:10.1021/acs.chemmater.7b01761 ISSN 0897-4756.
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Official URL: http://dx.doi.org/10.1021/acs.chemmater.7b01761
Abstract
High energy X-ray diffraction is used to follow in situ the crystallization of a cobalt gallate from metallic gallium under solvothermal conditions in an aminoalcohol, revealing the formation and decay of transient metastable layered double hydroxides. Photocatalytic studies show the spinel product has activity as a water oxidation catalyst for oxygen evolution.
Item Type: | Journal Article | ||||||||||||
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Subjects: | Q Science > QD Chemistry | ||||||||||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||||||||||
Library of Congress Subject Headings (LCSH): | Cobalt , Gallates, Gallium, Hydroxides | ||||||||||||
Journal or Publication Title: | Chemistry of Materials | ||||||||||||
Publisher: | American Chemical Society | ||||||||||||
ISSN: | 0897-4756 | ||||||||||||
Official Date: | 6 June 2017 | ||||||||||||
Dates: |
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Volume: | 29 | ||||||||||||
Number: | 12 | ||||||||||||
Page Range: | pp. 5053-5057 | ||||||||||||
DOI: | 10.1021/acs.chemmater.7b01761 | ||||||||||||
Status: | Peer Reviewed | ||||||||||||
Publication Status: | Published | ||||||||||||
Access rights to Published version: | Open Access (Creative Commons) | ||||||||||||
Date of first compliant deposit: | 12 June 2017 | ||||||||||||
Date of first compliant Open Access: | 25 July 2017 | ||||||||||||
RIOXX Funder/Project Grant: |
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