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Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides

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Cook, Daniel Sean, Wu, Yue, Lienau, Karla, More, Rene, Kashtiban, Reza J., Magdysyuk, Oxana V., Patzke, Greta R. and Walton, Richard I. (2017) Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides. Chemistry of Materials, 29 (12). pp. 5053-5057. doi:10.1021/acs.chemmater.7b01761

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Official URL: http://dx.doi.org/10.1021/acs.chemmater.7b01761

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Abstract

High energy X-ray diffraction is used to follow in situ the crystallization of a cobalt gallate from metallic gallium under solvothermal conditions in an aminoalcohol, revealing the formation and decay of transient metastable layered double hydroxides. Photocatalytic studies show the spinel product has activity as a water oxidation catalyst for oxygen evolution.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science > Chemistry
Library of Congress Subject Headings (LCSH): Cobalt , Gallates, Gallium, Hydroxides
Journal or Publication Title: Chemistry of Materials
Publisher: American Chemical Society
ISSN: 0897-4756
Official Date: 6 June 2017
Dates:
DateEvent
6 June 2017Available
6 June 2017Accepted
Volume: 29
Number: 12
Page Range: pp. 5053-5057
DOI: 10.1021/acs.chemmater.7b01761
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Open Access
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
CASE studentship[EPSRC] Engineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
URPP LightChECUniversität Zürichhttp://dx.doi.org/10.13039/501100006447
CRSII2_160801/1Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschunghttp://dx.doi.org/10.13039/501100001711
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