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Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides
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Cook, Daniel Sean, Wu, Yue, Lienau, Karla, More, Rene, Kashtiban, Reza J., Magdysyuk, Oxana V., Patzke, Greta R. and Walton, Richard I. (2017) Time-resolved powder X-ray diffraction of the solvothermal crystallization of cobalt gallate spinel photocatalyst reveals transient layered double hydroxides. Chemistry of Materials, 29 (12). pp. 5053-5057. doi:10.1021/acs.chemmater.7b01761
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WRAP-time-resolved-powder-X‑ray-diffraction-solvothermal-Walton-2017.pdf - Published Version - Requires a PDF viewer. Available under License Creative Commons Attribution 4.0. Download (2280Kb) | Preview |
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WRAP-time-resolved-powder-cobalt-hydroxides-Cook-2017.pdf - Accepted Version - Requires a PDF viewer. Download (828Kb) | Preview |
Official URL: http://dx.doi.org/10.1021/acs.chemmater.7b01761
Abstract
High energy X-ray diffraction is used to follow in situ the crystallization of a cobalt gallate from metallic gallium under solvothermal conditions in an aminoalcohol, revealing the formation and decay of transient metastable layered double hydroxides. Photocatalytic studies show the spinel product has activity as a water oxidation catalyst for oxygen evolution.
| Item Type: | Journal Article | ||||||||||||
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| Subjects: | Q Science > QD Chemistry | ||||||||||||
| Divisions: | Faculty of Science > Chemistry | ||||||||||||
| Library of Congress Subject Headings (LCSH): | Cobalt , Gallates, Gallium, Hydroxides | ||||||||||||
| Journal or Publication Title: | Chemistry of Materials | ||||||||||||
| Publisher: | American Chemical Society | ||||||||||||
| ISSN: | 0897-4756 | ||||||||||||
| Official Date: | 6 June 2017 | ||||||||||||
| Dates: |
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| Volume: | 29 | ||||||||||||
| Number: | 12 | ||||||||||||
| Page Range: | pp. 5053-5057 | ||||||||||||
| DOI: | 10.1021/acs.chemmater.7b01761 | ||||||||||||
| Status: | Peer Reviewed | ||||||||||||
| Publication Status: | Published | ||||||||||||
| Access rights to Published version: | Open Access | ||||||||||||
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