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Time resolved operando X-ray techniques in catalysis, a case study : CO oxidation by O2 over Pt surfaces and alumina supported Pt catalysts

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Newton, Mark E. (2017) Time resolved operando X-ray techniques in catalysis, a case study : CO oxidation by O2 over Pt surfaces and alumina supported Pt catalysts. Catalysts, 7 (2). 58. doi:10.3390/catal7020058

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Official URL: http://dx.doi.org/10.3390/catal7020058

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Abstract

The catalytic oxidation of CO by O2 to form CO2 over Pt surfaces and supported catalysts is one of the most studied catalytic reactions from both fundamental and applied points of view. This review aims to show how the application of a range of time resolved, X-ray based techniques, such as X-ray diffraction (XRD), Surface X-ray diffraction (SXRD), total X-ray scattering/pair distribution function (PDF), X-ray absorption (XAFS), X-ray emission (XES), and X-ray photoelectron spectroscopies (XPS), applied under operando conditions and often coupled to adjunct techniques (for instance mass spectrometry (MS) and infrared spectroscopy (IR)) have shed new light on the structures and mechanisms at work in this most studied of systems. The aim of this review is therefore to demonstrate how a fusion of the operando philosophy with the ever augmenting capacities of modern synchrotron sources can lead to new insight and catalytic possibilities, even in the case of a process that has been intensely studied for almost 100 years. View Full-Text

Item Type: Journal Article
Divisions: Faculty of Science > Physics
Journal or Publication Title: Catalysts
Publisher: MDPI
ISSN: 2073-4344
Official Date: 14 February 2017
Dates:
DateEvent
14 February 2017Published
26 January 2017Accepted
Volume: 7
Number: 2
Article Number: 58
DOI: 10.3390/catal7020058
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Open Access

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