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Confined crystallization of organic materials in nanopipettes : tracking the early stages of crystal growth and making seeds for unusual polymorphs

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Maddar, Faduma, Perry, David and Unwin, Patrick R. (2017) Confined crystallization of organic materials in nanopipettes : tracking the early stages of crystal growth and making seeds for unusual polymorphs. Crystal Growth & Design, 17 (12). pp. 6565-6571. doi:10.1021/acs.cgd.7b01224 ISSN 1528-7483.

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Official URL: http://dx.doi.org/10.1021/acs.cgd.7b01224

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Abstract

Nanopipettes are used as nanoreactors to study the crystallization of bicalutamide, in a nanoscale antisolvent configuration. Potential controlled ion migration is used to mix an aqueous solution and a dimethyl sulfoxide phase containing bicalutamide, inducing crystallization at the nanopore interface, and generating current blockades due to the nucleation and growth of crystal seeds.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science, Engineering and Medicine > Science > Chemistry
Library of Congress Subject Headings (LCSH): Crystallization , Crystal growth, Nanochemistry
Journal or Publication Title: Crystal Growth & Design
Publisher: American Chemical Society
ISSN: 1528-7483
Official Date: 6 December 2017
Dates:
DateEvent
6 December 2017Published
13 November 2017Available
13 November 2017Accepted
Volume: 17
Number: 12
Page Range: pp. 6565-6571
DOI: 10.1021/acs.cgd.7b01224
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Date of first compliant deposit: 22 November 2017
Date of first compliant Open Access: 13 November 2018
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
UNSPECIFIEDAstraZenecahttp://dx.doi.org/10.13039/100004325
UNSPECIFIEDEngineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
UNSPECIFIEDLeverhulme Trusthttp://dx.doi.org/10.13039/501100000275
Wolfson Research Merit AwardRoyal Societyhttp://dx.doi.org/10.13039/501100000288
UNSPECIFIEDUniversity of Warwick. Molecular Organisation and Assembly in Cells (MOAC)UNSPECIFIED

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