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Synthesis, characterisation and molecular structure of a calcium stannyl derivative [Ca{Sn(mu-OSiMe2But)(3)}(2)]
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UNSPECIFIED (2000) Synthesis, characterisation and molecular structure of a calcium stannyl derivative [Ca{Sn(mu-OSiMe2But)(3)}(2)]. MAIN GROUP METAL CHEMISTRY, 23 (8). pp. 395-400. ISSN 0334-7575.
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Abstract
The compound, [Ca{Sn(mu-OSiMe2But)(3)}(2)] 1, was prepared by the condensation reaction of Ca(OSiMe2But)(2) with Sn(OSiMe2But)(2) in dme. The structural characterisation revealed that 1 crystallises in the monoclinic system {Space group P2(1)/n (non-standard N-o 14)}. Each of the two Sn(mu-OSiMe2But)(3) anion binds the Ca(II) cation in an eta(6) fashion [av. Ca - O 2.408 Angstrom ]. Multinuclear [C-13, Si-29 and Sn-119 ] solid-state NMR spectroscopic studies are also reported. Compound 1 showed satisfactory elemental analysis.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | MAIN GROUP METAL CHEMISTRY | ||||
Publisher: | FREUND PUBLISHING HOUSE LTD | ||||
ISSN: | 0334-7575 | ||||
Official Date: | 2000 | ||||
Dates: |
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Volume: | 23 | ||||
Number: | 8 | ||||
Number of Pages: | 6 | ||||
Page Range: | pp. 395-400 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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