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Synthesis and structural characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] {Cp-S = C5Me4(SiMe2But)}
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UNSPECIFIED (2000) Synthesis and structural characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] {Cp-S = C5Me4(SiMe2But)}. MAIN GROUP METAL CHEMISTRY, 23 (5). pp. 307-310. ISSN 0334-7575.
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Abstract
The preparation and characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] 1 obtained by reacting [Pb(eta-Cp-S)(2)] with HOSO2CF3 is described in this paper [Cp-S = C5Me4(SiMe2Bu1)]. The single crystal X-ray study revealed that 1 exists as a polyionic species formed by the aggregation of four molecules of Pb(eta-Cp-S)(+) with one of Pb(OSO2CF3)(6)(4-). Compound 1 was micro-analyzed and studied by solution-state multinuclear NMR spectroscopy and the results are presented and discussed.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | MAIN GROUP METAL CHEMISTRY | ||||
Publisher: | FREUND PUBLISHING HOUSE LTD | ||||
ISSN: | 0334-7575 | ||||
Official Date: | May 2000 | ||||
Dates: |
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Volume: | 23 | ||||
Number: | 5 | ||||
Number of Pages: | 4 | ||||
Page Range: | pp. 307-310 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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