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The square-pyramidal Pd-II complex of a cross-bridged tetraazamacrocycle
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UNSPECIFIED (1999) The square-pyramidal Pd-II complex of a cross-bridged tetraazamacrocycle. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 55 (Part 9). pp. 1404-1406. ISSN 0108-2701.
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Abstract
The preparation and crystal structure of chloro(4,11-dimethyl-1,4, 8,11-tetraazabicyclo[6.6.2]hexadecane-kappa(4)N)palladium(II) chloride dihydrate, [PdCl(C14H30N4)]CI . 2H(2)O, are described. The Pd-II ion is coordinated to all four N atoms of the folded macrobicycle and to a single chloride ligand in a square-pyramidal geometry. The bond to the axial N atom is considerably longer than the others [Pd-N-ax 2.461 (3) and average Pd-N-eq 2.097 (10) Angstrom]. The Pd-Cl distance is 2.3407 (10) Angstrom.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | ||||
Publisher: | MUNKSGAARD INT PUBL LTD | ||||
ISSN: | 0108-2701 | ||||
Official Date: | 15 September 1999 | ||||
Dates: |
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Volume: | 55 | ||||
Number: | Part 9 | ||||
Number of Pages: | 3 | ||||
Page Range: | pp. 1404-1406 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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