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Developing B-11 solid state MAS NMR methods to characterise medium range structure in borates
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Barrow, Nathan S., Ashbrook, Sharon E., Brown, Steven P. and Holland, Diane (2009) Developing B-11 solid state MAS NMR methods to characterise medium range structure in borates. Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B, Vol.50 (No.3). pp. 201-204.
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Abstract
B-11 magic angle spinning solid state NMR spectra of polycrystalline lithium diborate are presented. Second order quadrupolar broadened resonances corresponding to three- (B3) and four-coordinated (B4) boron nuclei overlap for a magnetic field of 7.05 T but are resolved for 14.1 T Cross peaks linking the B3 and B4 resonances are observed in two-dimensional homonuclear spin diffusion spectra. There is a need to develop analytical methods for the characterisation of medium range structure in borate glasses. In this respect, such solid state NMR methods have potential or identifying the presence of specific superstructural units.
Item Type: | Journal Item | ||||
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Subjects: | Q Science > QD Chemistry T Technology > TP Chemical technology |
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Physics and Chemistry of Glasses - European Journal of Glass Science and Technology Part B | ||||
Publisher: | Society of Glass Technology | ||||
ISSN: | 1753-3562 | ||||
Official Date: | June 2009 | ||||
Dates: |
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Volume: | Vol.50 | ||||
Number: | No.3 | ||||
Number of Pages: | 4 | ||||
Page Range: | pp. 201-204 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access | ||||
Funder: | Engineering and Physical Sciences Research Council (EPSRC) | ||||
Grant number: | EP/D080355/1 (EPSRC) |
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