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Single-crystal K-x(ZnyTi8-y)O-16 priderites: Growth and characterization
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UNSPECIFIED (1996) Single-crystal K-x(ZnyTi8-y)O-16 priderites: Growth and characterization. JOURNAL OF MATERIALS SCIENCE, 31 (24). pp. 6463-6468. ISSN 0022-2461.
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Abstract
Single crystals of K-x(ZnyTi8-y)O-16 priderites have been grown from a melt of K2O-MoO3 using the flux-zone technique. High-purity crystals > 10 mm in length were obtained, with no indication of twinning. Lattice parameters of a=1.0162(8) nm and c=0.2971(7) nm were obtained from X-ray diffraction measurements. Habit planes were identified from scanning electron microscope images. X-ray photoelectron spectroscopy confirmed the titanium oxidation state as +4. High-temperature complex impedance spectroscopy between 300 and 820 K was used to electrically characterize the crystals. This indicated that the materials had a low d.c. conductivity and a conductivity of 1.68 x 10(-3) S cm(-1) at 100 kHz.
Item Type: | Journal Article | ||||
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Subjects: | T Technology > TA Engineering (General). Civil engineering (General) | ||||
Journal or Publication Title: | JOURNAL OF MATERIALS SCIENCE | ||||
Publisher: | CHAPMAN HALL LTD | ||||
ISSN: | 0022-2461 | ||||
Official Date: | 15 December 1996 | ||||
Dates: |
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Volume: | 31 | ||||
Number: | 24 | ||||
Number of Pages: | 6 | ||||
Page Range: | pp. 6463-6468 | ||||
Publication Status: | Published |
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