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A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite
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Laurencin, Danielle, Wong, Alan, Hanna, John V., Dupree, Ray and Smith, Mark E. (2008) A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite. Journal of the American Chemical Society, Vol.130 (No.8). pp. 2412-2413. doi:10.1021/ja710557t ISSN 0002-7863.
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Official URL: http://dx.doi.org/10.1021/ja710557t
Abstract
High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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Library of Congress Subject Headings (LCSH): | Hydroxyapatite, Nuclear magnetic resonance spectroscopy, Solid state chemistry, Calcium -- Analysis | ||||
Journal or Publication Title: | Journal of the American Chemical Society | ||||
Publisher: | American Chemical Society | ||||
ISSN: | 0002-7863 | ||||
Official Date: | 27 February 2008 | ||||
Dates: |
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Volume: | Vol.130 | ||||
Number: | No.8 | ||||
Number of Pages: | 2 | ||||
Page Range: | pp. 2412-2413 | ||||
DOI: | 10.1021/ja710557t | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access | ||||
Funder: | Sixth Framework Programme (European Commission) (FP6), Biotechnology and Biological Sciences Research Council (Great Britain) (BBSRC), Natural Sciences and Engineering Research Council of Canada (NSERC), Engineering and Physical Sciences Research Council (EPSRC), University of Warwick |
Data sourced from Thomson Reuters' Web of Knowledge
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