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Gas-phase methylation of [60]Fullerene
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Vieira, S. M. C., Drewello, T., Kotsiris, S. G., Rego, C. A. and Birkett, P. R. (2007) Gas-phase methylation of [60]Fullerene. Journal of Physical Chemistry B, Vol.111 (No.35). pp. 10352-10356. doi:10.1021/jp0733623 ISSN 1520-6106.
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Official URL: http://dx.doi.org/10.1021/jp0733623
Abstract
Direct methylation of [60]fullerene via a gas-phase reaction in a CH4/H-2 atmosphere was performed using a modified hot filament chemical vapor deposition method. Pressures were varied from 10 to 60 mbar and the substrate was maintained at 690 degrees C. High-resolution matrix-assisted laser desorption ionization (MALDI) mass spectrometry analysis showed signals corresponding to C60H18-2n(H,CH3)(n). Collision-induced dissociation experiments confirmed a maximum of 18 ligands possible to the [60]fullerene cage.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||
Journal or Publication Title: | Journal of Physical Chemistry B | ||||
Publisher: | American Chemical Society | ||||
ISSN: | 1520-6106 | ||||
Official Date: | 6 September 2007 | ||||
Dates: |
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Volume: | Vol.111 | ||||
Number: | No.35 | ||||
Number of Pages: | 5 | ||||
Page Range: | pp. 10352-10356 | ||||
DOI: | 10.1021/jp0733623 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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