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Identifying the intermolecular hydrogen-bonding supramolecular synthons in an indomethacin–nicotinamide cocrystal by solid-state NMR
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Maruyoshi, K., Iuga, Dinu, Antzutkin, Oleg N., Alhalaweh, Amjad, Velaga, Sitaram P. and Brown, Steven P. (2012) Identifying the intermolecular hydrogen-bonding supramolecular synthons in an indomethacin–nicotinamide cocrystal by solid-state NMR. Chemical Communications, Vol. 48 (No. 88). p. 10844. doi:10.1039/c2cc36094b ISSN 1359-7345.
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Official URL: http://dx.doi.org/10.1039/C2CC36094B
Abstract
Two-dimensional 1H double-quantum and 14N–1H & 1H–13C heteronuclear magic-angle spinning (MAS) NMR spectra recorded at natural isotopic abundance identify specific intermolecular COOHNarom and CHaromOC hydrogen-bonding interactions in the solid-state structure of an indomethacin–nicotinamide cocrystal, thus additionally proving cocrystal formation.
Item Type: | Journal Article | ||||
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Chemical Communications | ||||
Publisher: | Royal Society of Chemistry | ||||
ISSN: | 1359-7345 | ||||
Official Date: | 2012 | ||||
Dates: |
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Volume: | Vol. 48 | ||||
Number: | No. 88 | ||||
Page Range: | p. 10844 | ||||
DOI: | 10.1039/c2cc36094b | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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