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Regiospecific high yield reductive coupling of diynes to give a luminescent rhodium complex
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UNSPECIFIED (2001) Regiospecific high yield reductive coupling of diynes to give a luminescent rhodium complex. CHEMICAL COMMUNICATIONS (24). pp. 2626-2627. ISSN 1359-7345.
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Abstract
Reaction of 2 equivalents of 1,4-bis(p-tolylethynyl)buta-1,3-diyne with [(PMe3)(4)Rh(-C equivalent to CSiMe3)] gives the unusual, highly luminescent mer, cis-[tris(trimethylphosphine)trimethylsilylethynyl-2,5-bis(p-tolylethynyl)-3,4-bis(p-tolyl)rhodacyclopenta-2,4-diene] 5 in quantitative yield which has been fully characterised by H-1 and P-31{H-1} NMR, IR, UV-VIS and luminescence spectroscopies, elemental analysis and single crystal X-ray diffraction.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | CHEMICAL COMMUNICATIONS | ||||
Publisher: | ROYAL SOC CHEMISTRY | ||||
ISSN: | 1359-7345 | ||||
Official Date: | 21 December 2001 | ||||
Dates: |
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Number: | 24 | ||||
Number of Pages: | 2 | ||||
Page Range: | pp. 2626-2627 | ||||
Publication Status: | Published |
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