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Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation
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Tanaka, Joji, Gurnani, Pratik, Cook, Alexander B., Häkkinen, Satu, Zhang, Junliang, Yang, Jie, Kerr, Andrew, Haddleton, David M., Perrier, Sébastien and Wilson, Paul (2019) Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation. Polymer Chemistry, 10 (10). pp. 1186-1191. doi:10.1039/C8PY01437J ISSN 1759-9954.
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WRAP-microscale-synthesis-multiblock-copolymers-ultrafast-RAFT-polymerisation-Wilson-2019.pdf - Accepted Version - Requires a PDF viewer. Download (1164Kb) | Preview |
Official URL: http://dx.doi.org/10.1039/C8PY01437J
Abstract
We demonstrate that ultrafast RAFT in the presence of air can be scaled down to 2 μL with good control using microvolume insert vials as the polymerisation vessel. By careful cooling and mixing of the sequential monomers, well-defined pentablock copolymers were generated with a final volume of 10 μL.
Item Type: | Journal Article | ||||||||||||||||||
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Subjects: | Q Science > QD Chemistry | ||||||||||||||||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||||||||||||||||
Library of Congress Subject Headings (LCSH): | Block copolymers, Addition polymerization, Fragmentation reactions | ||||||||||||||||||
Journal or Publication Title: | Polymer Chemistry | ||||||||||||||||||
Publisher: | Royal Society of Chemistry | ||||||||||||||||||
ISSN: | 1759-9954 | ||||||||||||||||||
Official Date: | 14 March 2019 | ||||||||||||||||||
Dates: |
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Volume: | 10 | ||||||||||||||||||
Number: | 10 | ||||||||||||||||||
Page Range: | pp. 1186-1191 | ||||||||||||||||||
DOI: | 10.1039/C8PY01437J | ||||||||||||||||||
Status: | Peer Reviewed | ||||||||||||||||||
Publication Status: | Published | ||||||||||||||||||
Access rights to Published version: | Restricted or Subscription Access | ||||||||||||||||||
Date of first compliant deposit: | 26 February 2019 | ||||||||||||||||||
Date of first compliant Open Access: | 7 February 2020 | ||||||||||||||||||
RIOXX Funder/Project Grant: |
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