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Data for Synthesis and reduction reactions of pyridones and 5-acyl-2-methoxypyridines
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Bisset, Alexander A., Dishington, Allan, Jones, Teyrnon C., Clarkson, Guy J. and Wills, Martin (2019) Data for Synthesis and reduction reactions of pyridones and 5-acyl-2-methoxypyridines. [Dataset]
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PDF (Experimental data)
ch-250419-wrap-change--supporting_information_for_alex_heterocyclic_reductions_paper_150414.pdf - Published Version - Requires a PDF viewer. Available under License Creative Commons Attribution 4.0. Download (5Mb) | Preview |
Official URL: http://wrap.warwick.ac.uk/116584
Abstract
The synthesis of a series of pyridones, from their 2-hydroxypyridine or 2-methoxypyridine precursors, is described, along with studies into their reductions to saturated heterocycles. A number of 5-acylpyridones were prepared and were evaluated as substrates for asymmetric transfer hydrogenation prior to conversion to saturated heterocycles. The enantioselective reduction of 5-acetyl-1-benzylpyrimidine-2,4(1H,3H)-dione is also described.
| Item Type: | Dataset | |||||||||
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| Subjects: | Q Science > QD Chemistry | |||||||||
| Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | |||||||||
| Type of Data: | Experimental data | |||||||||
| Library of Congress Subject Headings (LCSH): | Organic compounds -- Synthesis, Hydroxypyridones -- Sythesis | |||||||||
| Publisher: | University of Warwick, Department of Chemistry | |||||||||
| Official Date: | 26 March 2019 | |||||||||
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| Status: | Peer Reviewed | |||||||||
| Publication Status: | Published | |||||||||
| Access rights to Published version: | Open Access (Creative Commons) | |||||||||
| Copyright Holders: | University of Warwick | |||||||||
| Description: | Supplemental information underpinning publication |
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| Date of first compliant deposit: | 28 December 2015 | |||||||||
| Date of first compliant Open Access: | 28 December 2015 | |||||||||
| Funder: | Engineering and Physical Sciences Research Council (EPSRC), AstraZeneca (Firm) | |||||||||
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