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Sol-gel synthesis and structure of borosilicon oxycarbide glasses
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UNSPECIFIED (1998) Sol-gel synthesis and structure of borosilicon oxycarbide glasses. JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 13 (1-3). pp. 1001-1004. ISSN 0928-0707.
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Abstract
Existing sol-gel polymerization/pyrolysis routes employing two separate boron containing metal alkoxide precursors have been applied to form multi-component silicon oxycarbide glasses based on a borosilicon oxycarbide (B-Si-O-C) system. Si-29 and B-11 magic angle spinning nuclear magnetic resonance (MAS-NMR) was used to characterize the atomic structure of the gels, glasses and glass ceramics. Structural changes such as glass formation and crystal nucleation were identified by X-ray diffraction (XRD). Transmission electron microscopy (TEM) provided images of crystal nucleation and growth.
Item Type: | Journal Article | ||||
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Subjects: | T Technology > TP Chemical technology | ||||
Journal or Publication Title: | JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY | ||||
Publisher: | KLUWER ACADEMIC PUBL | ||||
ISSN: | 0928-0707 | ||||
Official Date: | 1998 | ||||
Dates: |
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Volume: | 13 | ||||
Number: | 1-3 | ||||
Number of Pages: | 4 | ||||
Page Range: | pp. 1001-1004 | ||||
Publication Status: | Published |
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