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In situ X‐ray scattering of the crystallisation of basic magnesium chlorides using a laboratory instrument
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Pickering, Katie S., Huband, Steven, Shafran, Kirill L. and Walton, Richard I. (2022) In situ X‐ray scattering of the crystallisation of basic magnesium chlorides using a laboratory instrument. Chemistry–Methods, 2 (9). e202200033. doi:10.1002/cmtd.202200033 ISSN 2628-9725.
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WRAP-In-situ-X‐ray-scattering-crystallisation-basic-magnesium-chlorides-2022.pdf - Published Version - Requires a PDF viewer. Available under License Creative Commons Attribution 4.0. Download (4Mb) | Preview |
Official URL: http://dx.doi.org/10.1002/cmtd.202200033
Abstract
A method for in situ monitoring of the crystallisation of basic magnesium chlorides using a laboratory-based SAXS (small angle X-ray scattering)/ WAXS (wide angle X-ray scattering) instrument is demonstrated. By simultaneous acquisition of SAXS/WAXS, time-resolved particle size and phase evolution information was obtained for crystallisation of Mg3Cl(OH)5 ⋅ 4 H2O. Comparison of SAXS and WAXS data provides new mechanistic insights into the formation of this material, from long-range crystallographic order to nanoscale particle size, highlighting the information laboratory instruments can provide.
Item Type: | Journal Article | ||||||||
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Subjects: | Q Science > QD Chemistry | ||||||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry Faculty of Science, Engineering and Medicine > Science > Physics |
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Library of Congress Subject Headings (LCSH): | Chemistry, Inorganic, Chlorides, Magnesium, Crystallization, X-ray crystallography, X-rays -- Diffraction | ||||||||
Journal or Publication Title: | Chemistry–Methods | ||||||||
Publisher: | Wiley-Blackwell Publishing Ltd. | ||||||||
ISSN: | 2628-9725 | ||||||||
Official Date: | September 2022 | ||||||||
Dates: |
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Volume: | 2 | ||||||||
Number: | 9 | ||||||||
Article Number: | e202200033 | ||||||||
DOI: | 10.1002/cmtd.202200033 | ||||||||
Status: | Peer Reviewed | ||||||||
Publication Status: | Published | ||||||||
Access rights to Published version: | Open Access (Creative Commons) | ||||||||
Copyright Holders: | © 2022 The Authors. Published by Wiley-VCH GmbH | ||||||||
Date of first compliant deposit: | 7 November 2022 | ||||||||
Date of first compliant Open Access: | 7 November 2022 |
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