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An X-ray diffraction and NMR study into the mechanism of zircon formation from aqueous sols
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UNSPECIFIED (1996) An X-ray diffraction and NMR study into the mechanism of zircon formation from aqueous sols. JOURNAL OF MATERIALS SCIENCE, 31 (22). pp. 5873-5876. ISSN 0022-2461.
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Abstract
Solid solutions of the formula Zr1-xSixO2 (x=0-0.5) were produced by an aqueous inorganic set-gel route. X-ray diffraction and solid state magic-angle spinning-nuclear magnetic resonance (MAS-NMR) were used to characterize the products at various calcination temperatures. The solubility limit of silica in zirconia at <950 degrees C was found to be similar to x=0.15 and that this amount stabilized the tetragonal zirconia phase to higher temperatures and inhibited the formation of zircon. With x=0.5, zircon formation was 70% at only 1100 degrees C.
Item Type: | Journal Article | ||||
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Subjects: | T Technology > TA Engineering (General). Civil engineering (General) | ||||
Journal or Publication Title: | JOURNAL OF MATERIALS SCIENCE | ||||
Publisher: | CHAPMAN HALL LTD | ||||
ISSN: | 0022-2461 | ||||
Official Date: | 15 November 1996 | ||||
Dates: |
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Volume: | 31 | ||||
Number: | 22 | ||||
Number of Pages: | 4 | ||||
Page Range: | pp. 5873-5876 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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