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Film before aggregates : an operando GISAXS study on electrochemically assisted surfactant assembly
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Moehl, Gilles E., Fitch, Samuel D., Cicvarić, Katarina, Han, Yisong, Huang, Ruomeng, Rawle, Jonathan, Shao, Li, Beanland, Richard, Bartlett, Philip N., Denuault, Guy and Hector, Andrew L. (2024) Film before aggregates : an operando GISAXS study on electrochemically assisted surfactant assembly. Nanoscale, 16 (8). pp. 4197-4204. doi:10.1039/d3nr05126a ISSN 2040-3364.
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Official URL: http://doi.org/10.1039/d3nr05126a
Abstract
The process of electrochemically assisted surfactant assembly was followed in real time by grazing incidence small angle X-ray scattering with the aim to deconvolute the formation of mesoporous silica film and unwanted porous particles. The X-ray technique proved to be useful for the characterisation of this process, as it takes place at a very dynamic, solid/liquid interface. This paper shows the electrochemically driven onset and evolution of silica/surfactant structures. Additional control experiments indicate the formation of vertically aligned structures without the use of an electric field, although it seems to be beneficial for increased pore ordering.
Item Type: | Journal Article | ||||||||
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||||||
SWORD Depositor: | Library Publications Router | ||||||||
Journal or Publication Title: | Nanoscale | ||||||||
Publisher: | Royal Society of Chemistry | ||||||||
ISSN: | 2040-3364 | ||||||||
Official Date: | 28 February 2024 | ||||||||
Dates: |
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Volume: | 16 | ||||||||
Number: | 8 | ||||||||
Page Range: | pp. 4197-4204 | ||||||||
DOI: | 10.1039/d3nr05126a | ||||||||
Status: | Peer Reviewed | ||||||||
Publication Status: | Published | ||||||||
Access rights to Published version: | Open Access (Creative Commons) | ||||||||
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