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LIGANDS DESIGNED TO IMPOSE TETRAHEDRAL COORDINATION - A CONVENIENT ROUTE TO AMINOETHYL AND AMINOPROPYL PENDANT ARM DERIVATIVES OF 1,5,9-TRIAZACYCLODODECANE
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UNSPECIFIED (1992) LIGANDS DESIGNED TO IMPOSE TETRAHEDRAL COORDINATION - A CONVENIENT ROUTE TO AMINOETHYL AND AMINOPROPYL PENDANT ARM DERIVATIVES OF 1,5,9-TRIAZACYCLODODECANE. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS (18). pp. 2755-2757. ISSN 0300-9246.
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Abstract
The macrocyclic ligands 1-(2-aminoethyl)- (L1) and 1-(3-aminopropyl)-1,5,9-triazacyclododecane (L2) have been synthesised from 2,4-dioxo-1,5,9-triazacyclododecane, and the complexes [ZnL1(OClO3)]ClO4 (trigonal bipyramidal) and [NiL2(NCS)2] (octahedral) characterised by X-ray crystallography; L1 and L2 form more stable complexes than do analogues bearing tertiary amino groups on the pendant arms, but allow higher co-ordination numbers.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS | ||||
Publisher: | ROYAL SOC CHEMISTRY | ||||
ISSN: | 0300-9246 | ||||
Official Date: | 21 September 1992 | ||||
Dates: |
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Number: | 18 | ||||
Number of Pages: | 3 | ||||
Page Range: | pp. 2755-2757 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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