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Recent advances in solid-state 25mg NMR spectroscopy
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Freitas, Jair C.C. and Smith, Mark E. (2012) Recent advances in solid-state 25mg NMR spectroscopy. Annual Reports on NMR Spectroscopy, Vol.75 . pp. 25-114. doi:10.1016/B978-0-12-397018-3.00002-8 ISSN 0066-4103.
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Official URL: http://dx.doi.org/10.1016/B978-0-12-397018-3.00002...
Abstract
In spite of the relatively unfavourable characteristics of the 25Mg nuclide for NMR experiments-such as low natural abundance, small magnetogyric ratio and sizeable quadrupolar broadening-there is increasing evidence that solid-state 25Mg NMR is a powerful tool for studies involving many different materials. Much of the recent boost in this field has been driven by instrumental improvements, such as the availability of high magnetic fields and fast-spinning speeds, as well as by the use of signal-enhancement methods developed in the past decade for half-integer spin quadrupolar nuclei. The most relevant advances in solid-state 25Mg NMR spectroscopy are reviewed here, including a detailed account of the use of signal-enhancement methods and of the more recent applications of first-principles calculations of 25Mg NMR parameters. Examples of the application of 25Mg solid-state NMR are given for different classes of materials, including organic compounds, oxide-based materials, glasses, alloys and intermetallic compounds. © 2012 Elsevier Ltd.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QC Physics | ||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Annual Reports on NMR Spectroscopy | ||||
Publisher: | Academic Press | ||||
ISSN: | 0066-4103 | ||||
Book Title: | Annual Reports on NMR Spectroscopy Volume 75 | ||||
Official Date: | 2012 | ||||
Dates: |
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Volume: | Vol.75 | ||||
Page Range: | pp. 25-114 | ||||
DOI: | 10.1016/B978-0-12-397018-3.00002-8 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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