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A comparative study of the structure of sodium borophosphates made by sol-gel and melt-quench methods
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Qiu, Dong, Martin, Richard A., Knowles, Jonathan C., Smith, Mark E. and Newport, Robert J. (2010) A comparative study of the structure of sodium borophosphates made by sol-gel and melt-quench methods. Journal of Non-Crystalline Solids, Vol.356 (No.9-10). pp. 490-494. doi:10.1016/j.jnoncrysol.2009.12.016 ISSN 0022-3093.
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Official URL: http://dx.doi.org/10.1016/j.jnoncrysol.2009.12.016
Abstract
The atomic scale structure of sodium borophosphates made by the sol-gel method is compared to those made by the melt-quench method. It is found that although the sol-gel generated materials have a higher tendency towards crystallization, they nevertheless show a qualitatively similar crystallization trend with composition to their melt-quench analogues; the progressive introduction of boron oxide into the phosphate network initially inhibits then promotes crystallization. At the composition associated with the most stable amorphous sodium borophosphate (20 mol% boron oxide), it is found that the atomic scale structure of the sol-gel synthesized network glass is almost identical to that of the corresponding melt-quenched one. (C) 2009 Elsevier B.V. All rights reserved.
Item Type: | Journal Article | ||||
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Subjects: | T Technology > TP Chemical technology T Technology > TA Engineering (General). Civil engineering (General) |
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Journal of Non-Crystalline Solids | ||||
Publisher: | Elsevier Science BV | ||||
ISSN: | 0022-3093 | ||||
Official Date: | 15 March 2010 | ||||
Dates: |
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Volume: | Vol.356 | ||||
Number: | No.9-10 | ||||
Number of Pages: | 5 | ||||
Page Range: | pp. 490-494 | ||||
DOI: | 10.1016/j.jnoncrysol.2009.12.016 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access | ||||
Funder: | Engineering and Physical Sciences Research Council (EPSRC) | ||||
Grant number: | EP/C004671 (EPSRC), EP/C004698 (EPSRC), EP/C515560 (EPSRC) |
Data sourced from Thomson Reuters' Web of Knowledge
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