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A multinuclear 1H, 13C and 11B solid-state MAS NMR study of 16- and 18-electron organometallic ruthenium and osmium carborane complexes
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Barry, Nicolas P. E., Kemp, Thomas F., Sadler, P. J. and Hanna, John V. (2014) A multinuclear 1H, 13C and 11B solid-state MAS NMR study of 16- and 18-electron organometallic ruthenium and osmium carborane complexes. Dalton Transactions, Volume 43 (Number 13). pp. 4945-4949. doi:10.1039/c3dt53589d ISSN 1477-9226.
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Official URL: http://dx.doi.org/10.1039/c3dt53589d
Abstract
The first 1H, 13C, 31P and 11B solid state MAS NMR studies of electron-deficient carborane-containing ruthenium and osmium complexes [Ru/Os(p-cym)(1,2-dicarba-closo-dodecaborane-1,2-dithiolate)] are reported. The MAS NMR data from these 16-electron complexes are compared to those of free carborane-ligand and an 18-electron triphenylphosphine ruthenium adduct, and reveal clear spectral differences between 16- and 18-electron organometallic carborane systems in the solid state.
Item Type: | Journal Article | ||||||||||
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry Faculty of Science, Engineering and Medicine > Science > Physics |
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Journal or Publication Title: | Dalton Transactions | ||||||||||
Publisher: | Royal Society of Chemistry | ||||||||||
ISSN: | 1477-9226 | ||||||||||
Official Date: | 7 April 2014 | ||||||||||
Dates: |
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Volume: | Volume 43 | ||||||||||
Number: | Number 13 | ||||||||||
Page Range: | pp. 4945-4949 | ||||||||||
DOI: | 10.1039/c3dt53589d | ||||||||||
Status: | Peer Reviewed | ||||||||||
Publication Status: | Published | ||||||||||
Access rights to Published version: | Restricted or Subscription Access |
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