The Library
The 2D MAS NMR spin-echo experiment: the determination of C-13-C-13 J couplings in a solid-state cellulose sample
Tools
UNSPECIFIED (2004) The 2D MAS NMR spin-echo experiment: the determination of C-13-C-13 J couplings in a solid-state cellulose sample. JOURNAL OF MAGNETIC RESONANCE, 171 (1). pp. 43-47. doi:10.1016/j.jmr.2004.07.022 ISSN 1090-7807.
Research output not available from this repository.
Request-a-Copy directly from author or use local Library Get it For Me service.
Official URL: http://dx.doi.org/10.1016/j.jmr.2004.07.022
Abstract
A simple C-13 MAS spin-echo experiment is applied to a partially C-13-labelled cellulose sample extracted from wood. C-13-C-13 J couplings are determined even though considerable chemical disorder leads to observed linewidths in the normal 1D C-13 CP MAS spectrum which far exceed the J couplings. The fitting of the experimental data also allows the quantification of the degree of isotopic enrichment. (C) 2004 Elsevier Inc. All rights reserved.
Item Type: | Journal Article | ||||
---|---|---|---|---|---|
Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
||||
Journal or Publication Title: | JOURNAL OF MAGNETIC RESONANCE | ||||
Publisher: | ACADEMIC PRESS INC ELSEVIER SCIENCE | ||||
ISSN: | 1090-7807 | ||||
Official Date: | November 2004 | ||||
Dates: |
|
||||
Volume: | 171 | ||||
Number: | 1 | ||||
Number of Pages: | 5 | ||||
Page Range: | pp. 43-47 | ||||
DOI: | 10.1016/j.jmr.2004.07.022 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
Request changes or add full text files to a record
Repository staff actions (login required)
View Item |